Solid-State NMR III Organic Matter
Title | Solid-State NMR III Organic Matter PDF eBook |
Author | Bernhard Blümich |
Publisher | Springer Science & Business Media |
Pages | 218 |
Release | 2012-12-06 |
Genre | Science |
ISBN | 3642612237 |
Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.
Solid-State NMR III Organic Matter
Title | Solid-State NMR III Organic Matter PDF eBook |
Author | Bernhard Blümich |
Publisher | Springer |
Pages | 0 |
Release | 2011-09-28 |
Genre | Science |
ISBN | 9783642647512 |
Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.
Solid-State NMR III Organic Matter
Title | Solid-State NMR III Organic Matter PDF eBook |
Author | |
Publisher | Springer |
Pages | 213 |
Release | 1994-11-04 |
Genre | Science |
ISBN | 9783540573999 |
Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.
Solid-State NMR III Organic Matter
Title | Solid-State NMR III Organic Matter PDF eBook |
Author | Bernhard Blümich |
Publisher | Springer |
Pages | 0 |
Release | 1994-11-04 |
Genre | Science |
ISBN | 9783540573999 |
Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.
Solid-State NMR I Methods
Title | Solid-State NMR I Methods PDF eBook |
Author | B. Blümich |
Publisher | Springer |
Pages | 282 |
Release | 1993-12-21 |
Genre | Science |
ISBN | 9783540571896 |
Solid-State NMR and Organic Geochemistry
Title | Solid-State NMR and Organic Geochemistry PDF eBook |
Author | Jingdong Mao |
Publisher | Elsevier |
Pages | 710 |
Release | 2021-11-15 |
Genre | Science |
ISBN | 9780128195741 |
Solid-State NMR and Organic Geochemistry explains solid-state NMR from the point of view of organic geochemists interested in applying solid-state NMR in their research. The book sets the scene in the first two chapters by describing the basic concepts of solid-state NMR adapted for non-NMR specialists as well as an overview of organic geochemistry for NMR specialists. The essentials for acquiring reliable spectra of complex organic matter are then described in Chapter 3. Chapter 4 introduces the systematic and advanced solid-state NMR techniques and approach to characterizing complex organic mixtures developed in Dr. Mao's laboratory. Practical aspects of performing solid-state NMR experiments of complex organic matter are discussed in Chapter 5. Chapters 6 through 15 are focused on applications of solid-state NMR in organic geochemistry, starting with geochemically important functional groups and biopolymers, followed by organic matter from soils, water, sediments, and aerosols, peat, coal, kerogen, and oil shale. The interactions of organic matter with organic contaminants probed by solid-state NMR are described in Chapter 16. Finally, the last chapter covers isotopic enrichment and labelling and solid-state NMR, and their applications in organic geochemistry. Bridges the gap between NMR specialists and organic geochemists, adapting solid-state NMR theory for non-NMR specialists Brings together NMR applications for a range of materials not often discussed in other NMR books, including applications to soil, aerosols, peat, coal, kerogen, and more Includes additional resources for further reading and problems to facilitate learning and application of key concepts in each chapter
Solid-state NMR Analysis of Soil Organic Matter Fractions from Integrated Physical-chemical Extraction
Title | Solid-state NMR Analysis of Soil Organic Matter Fractions from Integrated Physical-chemical Extraction PDF eBook |
Author | Xiaoyan Cao |
Publisher | |
Pages | 11 |
Release | 2011 |
Genre | Extraction (Chemistry) |
ISBN |