Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition)
Title | Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) PDF eBook |
Author | Peter Kusch |
Publisher | World Scientific |
Pages | 383 |
Release | 2023-08-28 |
Genre | Science |
ISBN | 1800613008 |
Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.
Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials
Title | Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials PDF eBook |
Author | Peter Kusch |
Publisher | World Scientific |
Pages | 267 |
Release | 2018-10-08 |
Genre | Science |
ISBN | 1786345773 |
The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.
Pyrolysis - GC/MS Data Book of Synthetic Polymers
Title | Pyrolysis - GC/MS Data Book of Synthetic Polymers PDF eBook |
Author | Shin Tsuge |
Publisher | Elsevier |
Pages | 406 |
Release | 2011-10-13 |
Genre | Performing Arts |
ISBN | 0444538925 |
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample
Introductory Chapter: Analytical Pyrolysis - Gas Chromatography/Mass Spectrometry of Polymeric Materials
Title | Introductory Chapter: Analytical Pyrolysis - Gas Chromatography/Mass Spectrometry of Polymeric Materials PDF eBook |
Author | Peter Kusch |
Publisher | |
Pages | |
Release | 2018 |
Genre | |
ISBN |
Pyrolysis Gas Chromatography of Some Polymeric Materials
Title | Pyrolysis Gas Chromatography of Some Polymeric Materials PDF eBook |
Author | Lena Trojer |
Publisher | |
Pages | 23 |
Release | 1981 |
Genre | |
ISBN |
Analytical Pyrolysis
Title | Analytical Pyrolysis PDF eBook |
Author | C.E.R. Jones |
Publisher | Elsevier |
Pages | 435 |
Release | 2012-12-02 |
Genre | Science |
ISBN | 0444601406 |
Analytical Pyrolysis presents the Proceedings of the Third International Symposium on Analytical Pyrolysis, held in Amsterdam on September 7-9, 1976. It looks at newly emergent techniques in analytical pyrolysis, including pyrolysis mass spectrometry, gas chromatography, thin-layer chromatography, and pyrolysis-gas liquid chromatography. The book also covers topics ranging from automation and microbiology to forensic science and pharmacology, reproducibility and specificity, biochemistry, laser-induced pyrolysis, pyrolytic reaction mechanisms, and polymers. Comprised of 50 chapters, this book begins with a discussion of automatic analysis of tire rubber blends using computer-linked pyrolysis gas chromatography, thermal procedures in coupling with thin-layer chromatography, the role of pyrolysis-gas liquid chromatography in biomedical studies, and the identification of microorganisms by pyrolysis gas-liquid chromatography. It then examines forensic applications of analytical pyrolysis techniques, structure and degradation behavior of synthetic polymers using pyrolysis in combination with field ion mass spectrometry, determination of polysaccharides in fulvic acids by pyrolysis gas chromatography, and application of Curie-point pyrolysis mass spectrometry in fungal taxonomy. The reader is also introduced to pyrolysis mass spectrometry of model compounds labeled with stable isotopes, the use of pyrolysis/gas chromatography to determine the quality of porous polymers of styrene cross-linked with divinyl benzene, and application of pyrohydrolysis for a rapid and accurate determination of halides in silicate rocks and minerals. This volume will benefit students, researchers, chemists, and scientists working in the field of analytical pyrolysis.
Applied Pyrolysis Handbook
Title | Applied Pyrolysis Handbook PDF eBook |
Author | Thomas P. Wampler |
Publisher | CRC Press |
Pages | 302 |
Release | 2006-12-13 |
Genre | Science |
ISBN | 1420017497 |
Analytical pyrolysis allows scientists to use routine laboratory instrumentation for analyzing complex, opaque, or insoluble samples more effectively than other analytical techniques alone. Applied Pyrolysis Handbook, Second Edition is a practical guide to the application of pyrolysis techniques to various samples and sample types for a dive