Physical Methods in Modern Chemical Analysis, Volume 3 presents the fundamental principles, the instrumentation or necessary equipment, and applications of selected physical methodologies in chemical analysis. This volume contains chapters that discuss various topics on chemical analysis methods such as transform methods in chemistry; X-ray spectrometry; the principles of electrochemical measurements; and global optimization strategy for gas-chromatographic separations. The book will prove to be an excellent reference material for chemists, researchers, and students of chemistry.

Physical Methods in Modern Chemical Analysis, Volume 2 covers the fundamental principles, the instrumentation or necessary equipment, and applications of selected physical methods. This volume contains five chapters, and deals first with the theory, instrumentation, column features, and applications of high-performance liquid chromatography. The next two chapters survey the principles, experimental aspects, procedures, and specific applications of X-ray photoelectron spectroscopy and X-ray diffraction methods. A chapter discusses the technical and theoretical aspects of ion cyclotron resonance, with a special emphasis on its application in gas phase ion and neutral compounds analysis. The last chapter explores the apparatus and experimental procedures in refractive index measurements. This book will be of value to analytical chemists and analytical chemistry researchers.

Physical Methods in Chemical Analysis, Volume III focuses on the application of physical methods in chemical analysis, including chromatography, spectroscopy, nuclear magnetic resonance, and photometry. The selection first offers information on gas chromatography, electrochromatography, and electroanalytical methods in trace analysis. Discussions focus on analytical applications, apparatus and techniques, titration methods, anodic stripping of deposited metals, and polarography. The book then examines the high-frequency method of chemical analysis, field emission microscopy, and theory and principles of sampling for chemical analysis. The publication takes a look at flame photometry and microwave spectroscopy. Topics include sample treatment required for flame photometric determinations; factors affecting precision and accuracy in flame photometry; theoretical background of microwave spectroscopy, and problems connected with quantitative analysis. The manuscript then elaborates on analytical applications of nuclear magnetic resonance; fluorescent x-ray spectrometric analysis; and neutron spectroscopy and neutron interactions in chemical analysis. The selection is a dependable reference for readers interested in the application of physical methods in chemical analysis.