Experimental Pulse NMR
Title | Experimental Pulse NMR PDF eBook |
Author | Eiichi Fukushima |
Publisher | CRC Press |
Pages | 556 |
Release | 2018-03-08 |
Genre | Science |
ISBN | 042996241X |
This book is about pulse nuclear magnetic resonance (NMR), with its techniques, the information to be obtained, and practical advice on performing experiments. The emphasis is on the motivation and physical ideas underlying NMR experiments and the actual techniques, including the hardware used. The level is generally suitable for those to whom pulse NMR is a new technique, be they students in chemistry or physics on the one hand and research workers in biology, geology, or agriculture, on the other. The book can be used for a senior or first year graduate course where it could supplement the standard NMR texts.
Experimental Pulse NMR
Title | Experimental Pulse NMR PDF eBook |
Author | Eiichi Fukushima |
Publisher | CRC Press |
Pages | 290 |
Release | 2018-03-08 |
Genre | Science |
ISBN | 0429973497 |
This book is about pulse nuclear magnetic resonance (NMR), with its techniques, the information to be obtained, and practical advice on performing experiments. The emphasis is on the motivation and physical ideas underlying NMR experiments and the actual techniques, including the hardware used. The level is generally suitable for those to whom pulse NMR is a new technique, be they students in chemistry or physics on the one hand and research workers in biology, geology, or agriculture, on the other. The book can be used for a senior or first year graduate course where it could supplement the standard NMR texts.
200 and More NMR Experiments
Title | 200 and More NMR Experiments PDF eBook |
Author | Stefan Berger |
Publisher | John Wiley & Sons |
Pages | 868 |
Release | 2004-07-02 |
Genre | Science |
ISBN | 3527310673 |
This work-book will guide you safely, in step-by-step descriptions, through every detail of the NMR experiments within, beginning with 1D routine experiments and ending with a series of advanced 3D experiments on a protein: ? Which experiment can best yield the desired information? ? How must the chosen experiment be performed? ? How does one read the required information from the spectrum? ? How does this particular pulse sequence work? ? Which other experiments give similar information? This third edition of the book, following its two highly successful predecessors, has been revised and expanded to 206 experiments. They are organized in 15 chapters, covering test procedures and routine spectra, variable temperature measurements, the use of auxiliary reagents, 1D multipulse experiments, spectra of heteronuclides, and the application of selective pulses. The second and third dimensions are introduced using pulsed field gradients, and experiments on solid state materials are described. A key part describes 3D experiments on the protein ubiquitin with 76 amino acids. What is new in this third edition? 1. 24 new experiments have been inserted into the 14 chapters that were in the 2nd edition, e.g., alpha/beta-SELINCOR-TOCSY, WET, DOSY, ct-COSY, HMSC, HSQC with adiabatic pulses, HETLOC. J-resolved HMBC, (1,1)- and (1,n)-ADEQUATE, STD, REDOR, and HR-MAS. 2. 20 new protein NMR experiments have been specially devised and are collected in the newly added Chapter 15, ProteinNMR, for which one needs a special model sample: fully 13C- and 15N-labeled human ubiquitin. Techniques used include the constant time principle, the PEP method, filters, gradient selection, and the echo/anti-echo procedure. The guide has been written by experts in this field, following the principle of learning by doing: all the experiments have been specially performed for this book, exactly as described and shown in the spectra that are reproduced. Being a reference source and work-book for the NMR laboratory as well as a textbook, it is a must for every scientist working with NMR, as well as for students preparing for their laboratory courses
Pulse and Fourier Transform NMR
Title | Pulse and Fourier Transform NMR PDF eBook |
Author | Thomas C. Farrar |
Publisher | Elsevier |
Pages | 132 |
Release | 2012-12-02 |
Genre | Science |
ISBN | 0080918123 |
Pulse and Fourier Transform NMR: Introduction to Theory and Methods presents the different types of pulse experiments that are commonly used and provides the theoretical background necessary for understanding these techniques. This book evaluates the practical application of pulse methods and the necessary instrumentation. Organized into seven chapters, this book begins with an overview of the NMR fundamentals and the basic pulse methods. This text then summarizes the important features of pulse spectrometers. Other chapters consider the rationale, the advantages, and the limitations of Fourier transform NMR methods. This book discusses as well how the idea of the rotating frame can be utilized to understand certain experiments that extend the range of application of pulse methods. The final chapter deals with a few significant special uses of pulse techniques. This book is a valuable resource for chemists and readers who are familiar with high resolution NMR but with no background in pulse methods.
50 and More Essential NMR Experiments
Title | 50 and More Essential NMR Experiments PDF eBook |
Author | Matthias Findeisen |
Publisher | John Wiley & Sons |
Pages | 322 |
Release | 2013-07-30 |
Genre | Science |
ISBN | 352733694X |
This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.
Multiple Pulse NMR Experiments
Title | Multiple Pulse NMR Experiments PDF eBook |
Author | Lee Michael Huber |
Publisher | |
Pages | 304 |
Release | 1968 |
Genre | |
ISBN |
NMR
Title | NMR PDF eBook |
Author | P. J. Hore |
Publisher | Oxford University Press, USA |
Pages | 133 |
Release | 2015 |
Genre | Science |
ISBN | 0198703422 |
This primer describes the range of NMR techniques commonly used in modern research, and explains how these experiments actually work, giving a unique perspective on this powerful experimental tool.