The objective of this thesis is to validate Resonant Ultrasound Spectroscopy (RUS) as a non-destructive evaluation tool that can be used to study effects of radiation on the mechanical properties of a material, mainly its elastic constants. RUS involves experimentally measuring the resonant frequencies of a sample and calculating the elastic constants based on these measurements. Finite Element Method (FEM) is used to get the frequencies of the modes of free vibration for the sample model. This result depends on the elastic constant values used in the FEM simulation. Studies were conducted to confirm the accuracy of the FEM model, and determine the right configuration and parameters to use for the simulation. Assuming uniform and isotropic elastic property changes, the effects of radiation damage can be quantified by obtaining a set of matching resonant frequencies between the experimental and FEM simulation results, before and after irradiating the sample. This is done by adjusting the elastic constant values used in the simulation so that the results match with the experimentally obtained resonant frequencies. With powerful enough equipment, even real time monitoring is possible in harsh environments, thus pointing out imminent failure.

The purpose of this thesis is to study Resonance Ultrasound Spectroscopy(RUS) and it's potential to evaluate the change in interfacial thermal resistance due to irradiation. Resonant Ultrasound Spectroscopy is conventionally used to determine the material properties of elastic bodies. It is a nondestructive technique that is very capable of extracting the elastic constants for a complete anisotropic material. Finite Element Method(FEM) is used to determine the natural frequency of a hollow cylinder. FEM was used due to the shape of the object. An experimental system was developed to capture the resonant frequencies of a hollow cylinder which is similar to Molybdenum-99 target. After successfully determining the resonance frequencies from the spectra, the frequencies were inverted to the elastic constants using the finite element model. Radiation effects on elastic constants was also studied. An investigation was made to assess the usefulness of RUS in evaluating radiation damage of materials. An experimental study was also completed to analyze the differences in RUS spectra in a contact pressure analysis between two cylinders of Molybdenum-99 target.

All objects exhibit vibrational resonances when mechanically excited. These resonant frequencies are determined by density, geometry, and elastic moduli. Resonant ultrasound spectroscopy (RUS) takes advantage of the known relationship between the parameters. In particular, for a freely suspended object, with three of the four parameters (vibrational spectra, density, geometry, or elastic moduli) known the remaining one can be calculated. From a materials characterization standpoint it is straight-forward to measure density and geometry but less so to measure all the elastic moduli. It has recently become possible to quickly and accurately measure vibrational spectra, and using code written at Los Alamos, calculate all the elastic moduli simultaneously. This is done to an accuracy of better than one percent for compression and 0.1 percent for shear. RUS provides rapid acquisition of materials information here-to-fore obtainable only with difficulty. It will greatly facilitate the use of real materials properties in models and thus make possible more realistic modeling results. The technique is sensitive to phase changes and microstructure. This offers a change to input real data into microstructure and phase change models. It will also enable measurement of moduli at locations in and about a weld thus providing information for a validating coupled thermomechanical calculations.

Metal additive manufacturing (AM) has started to overshadow traditional manufacturing practices thanks to its ability to produce complex, high-performance and application-customized components. However, AM process parameters have not been optimized, leading to inconsistencies and imperfections such as cracks and pores in parts, as well as deviations from the original design. Nondestructive evaluation (NDE) methods used for part qualification such as x-ray computed tomography (CT) and conventional ultrasonic testing (UT) have limitations in their abilities. X-ray CT is costly, hazardous, and offers limited resolution for larger components while many UT methods have limited applicability for inspection of parts with complex geometries or rough surfaces. Here, we conduct an integrated numerical and experimental study to investigate the feasibility of resonance ultrasound spectroscopy (RUS) as an alternative NDE method to inspect complex AM lattice structures with a varying number of missing struts. The most encouraging results are obtained when test samples have traction-free boundary conditions. The results of numerical simulations including eigenfrequency and frequency domain analyses are promising, indicating that the pristine and defective lattice samples should theoretically be distinguishable. In addition, given a reference intact sample, characterizing the extent of the defect in terms of the number of missing struts appears feasible. We introduce a similarity metric to compare the spectra after being locally normalized. However, the experimental results are not as conclusive. Although pristine and defective lattices may be distinguished for some cases, the number of missing struts cannot be inferred. The discrepancies between the numerical and experimental results are likely due to our simplified assumptions about material properties in numerical simulations and/or the presence of other unaccounted defects and heterogeneities in test samples.

This thesis demonstrates the practicability of using Resonant Ultrasound Spectroscopy (RUS) in combination with Finite Element Analysis (FEA) to determine the size and location of a defect in a material of known geometry and physical constants. Defects were analyzed by comparing the actual change in frequency spectrum measured by RUS to the change in frequency spectrum calculated using FEA. FEA provides a means of determining acceptance/rejection criteria for Non-Destructive Testing (NDT). If FEA models of the object are analyzed with defects in probable locations; the resulting resonant frequency spectra will match the frequency spectra of actual objects with similar defects. By analyzing many FEA-generated frequency spectra, it is possible to identify patterns in behavior of the resonant frequencies of particular modes based on the nature of the defect (location, size, depth, etc.). Therefore, based on the analysis of sufficient FEA models, it should be possible to determine nature of defects in a particular object from the measured resonant frequency. Experiments were conducted on various materials and geometries comparing resonant frequency spectra measured using RUS to frequency spectra calculated using FEA. Measured frequency spectra matched calculated frequency spectra for steel specimens both before and after introduction of a thin cut. Location and depth of the cut were successfully identified based on comparison of measured to calculated resonant frequencies. However, analysis of steel specimens with thin cracks, and of ceramic specimens with thin cracks, showed significant divergence between measured and calculated frequency spectra. Therefore, it was not possible to predict crack depth or location for these specimens. This thesis demonstrates that RUS in combination with FEA can be used as an NDT method for detection and analysis of cracks in various materials, and for various geometries, but with some limitations. Experimental results verify that cracks can be detected, and their depth and location determined with reasonable accuracy. However, experimental results also indicate that there are limits to the applicability of such a method, the primary one being a lower limit to the size of crack - especially thickness of the crack - for which this method can be applied.

Updated, revised, and restructured to reflect the latest advances in science and applications, the fourth edition of this best-selling industry and research reference covers the fundamental physical acoustics of ultrasonics and transducers, with a focus on piezoelectric and magnetostrictive modalities. It then discusses the full breadth of ultrasonics applications involving low power (sensing) and high power (processing) for research, industrial, and medical use. This book includes new content covering computer modeling used for acoustic and elastic wave phenomena, including scattering, mode conversion, transmission through layered media, Rayleigh and Lamb waves and flexural plates, modern horn design tools, Langevin transducers, and material characterization. There is more attention on process monitoring and advanced nondestructive testing and evaluation (NDT/NDE), including phased array ultrasound (PAUT), long-range inspection, using guided ultrasonic waves (GUW), internally rotary inspection systems (IRIS), time-of-flight diffraction (TOFD), and acoustic emission (AE). These methods are discussed and applied to both metals and nonmetals using illustrations in various industries, including now additionally for food and beverage products. The topics of defect sizing, capabilities, and limitations, including the probability of detection (POD), are introduced. Three chapters provide a new treatment of high-power ultrasonics, for both fluids and solids, and again, with examples of industrial engineering, food and beverage, pharmaceuticals, petrochemicals, and other process applications. Expanded coverage is given to medical and biological applications, covering diagnostics, therapy, and, at the highest powers, surgery. Key Features Provides an overview of fundamental analysis and transducer technologies needed to design and develop both measurement and processing systems Considers applications in material characterization and metrology Covers ultrasonic nondestructive testing and evaluation and high-power ultrasonics, which involves interactions that change the state of material Highlights medical and biomedical applications of ultrasound, focusing on the physical acoustics and the technology employed for diagnosis, therapy, surgery, and research This book is intended for both the undergraduate and graduate scientists and engineers, as well as the working professional, who seeks to understand the fundamentals together with a holistic treatment of the field of ultrasonics and its diversity of applications.