The basics and principles of new electrochemical methods and also their usage for fabrication and analysis of different nanostructures were discussed in this book. These methods consist of electrochemical methods in nanoscale (e.g. electrochemical atomic force microscopy and electrochemical scanning tunneling microscopy) and also electrochemical methods for fabrication of nanomaterials.

This book summarizes the electrochemical routes of nanostructure preparation in a systematic and didactic manner. It provides a comprehensive overview of electrodeposition, anodization, carbon nanotube preparation and other methods of nanostructure fabrication, combining essential information on the physical background of electrochemistry with materials science aspects of the field. The book includes a brief introduction to general electrochemistry with an emphasis on physico-chemical aspects, followed by a description of the sample preparation methods. In each chapter, an overview of the particular method is accompanied by a discussion of the relevant physical or chemical properties of the materials, including magnetic, mechanical, optical, catalytic, sensoric and other features. While some preparation methods are discussed in connection with the theories of physical electrochemistry (e.g. electrodeposition), the book also covers methods that are more heuristic but nonetheless utilize electric current (e.g. anodization of porous alumina or synthesis of carbon nanotubes by means of electric arc discharge).

Characterization of Nanomaterials: Advances and Key Technologies discusses the latest advancements in the synthesis of various types of nanomaterials. The book's main objective is to provide a comprehensive review regarding the latest advances in synthesis protocols that includes up-to-date data records on the synthesis of all kinds of inorganic nanostructures using various physical and chemical methods. The synthesis of all important nanomaterials, such as carbon nanostructures, Core-shell Quantum dots, Metal and metal oxide nanostructures, Nanoferrites, polymer nanostructures, nanofibers, and smart nanomaterials are discussed, making this a one-stop reference resource on research accomplishments in this area. Leading researchers from industry, academia, government and private research institutions across the globe have contributed to the book. Academics, researchers, scientists, engineers and students working in the field of polymer nanocomposites will benefit from its solutions for material problems. - Provides an up-to-date data record on the synthesis of all kinds of organic and inorganic nanostructures using various physical and chemical methods - Presents the latest advances in synthesis protocols - Presents latest techniques used in the physical and chemical characterization of nanomaterials - Covers characterization of all the important materials groups such as: carbon nanostructures, core-shell quantumdots, metal and metal oxide nanostructures, nanoferrites, polymer nanostructures and nanofibers - A broad range of applications is covered including the performance of batteries, solar cells, water filtration, catalysts, electronics, drug delivery, tissue engineering, food packaging, sensors and fuel cells - Leading researchers from industry, academia, government and private research institutes have contributed to the books

This completely updated and expanded second edition stands as a comprehensive knowledgebase on both the fundamentals and applications of this important materials processing method. The diverse, international team of contributing authors of this reference clarify in extensive detail properties and applications of sol-gel science and technology as it pertains to the production of substances, active and non-active, including optical, electronic, chemical, sensor, bio- and structural materials. Essential to a wide range of manufacturing industries, the compilation divides into the three complementary sections: Sol-Gel Processing, devoted to general aspects of processing and recently developed materials such as organic-inorganic hybrids, photonic crystals, ferroelectric coatings, and photocatalysts; Characterization of Sol-Gel Materials and Products, presenting contributions that highlight the notion that useful materials are only produced when characterization is tied to processing, such as determination of structure by NMR, in-situ characterization of the sol-gel reaction process, determination of microstructure of oxide gels, characterization of porous structure of gels by the surface measurements, and characterization of organic-inorganic hybrid; and Applications of Sol-Gel Technology, covering applications such as the sol-gel method used in processing of bulk silica glasses, bulk porous gels prepared by sol-gel method, application of sol-gel method to fabrication of glass and ceramic fibers, reflective and antireflective coating films, application of sol-gel method to formation of photocatalytic coating films, and application of sol-gel method to bioactive coating films. The comprehensive scope and integrated treatment of topics make this reference volume ideal for R&D scientists and engineers across a wide range of disciplines and professional interests.

Carbon Nanomaterials-Based Sensors: Emerging Research Trends in Devices and Applications covers the most recent research and design trends for carbon nanomaterials-based sensors for a variety of applications, including clinical and environmental uses, and more. Carbon nanomaterials-based sensors can be used with high sensitivity, stability and accuracy compared to other techniques. Written by experts in their given fields from around the world, this book helps researchers solve the particular challenges they face when developing new types of sensors. It instructs how to make sensitive, selective, robust, fast-response and stable carbon nanomaterial-based sensors, as well as how to utilize them in real life. - Covers the environmental monitoring and analytical implications of electro-analytical methods, one of the most dynamically developing branches of carbon nanomaterials - Includes a complete discussion of functionalized nanostructure materials reformulated with noble materials and advanced characteristics for improved applications when compared to standard materials - Covers sustainability and challenges in the commercialization of carbon nanomaterials-based sensors

Photoelectrochemical processes due to the symbiosis of photochemical and electrochemical processes result in unique reaction pathways and products. This technique catalysed by nanomaterials is extensively used to harness sunlight for production of fuels and chemical feedstocks. This book explains the basic concepts of photoelectrochemistry as well as their application in the generation of solar fuels from water, CO2 and N2 as feedstocks. It also contains standard methodologies and benchmarks of fuel production including current state of the art in nanocatalysts as well as their mechanism of action. This book: Explores fundamentals and real-time applications of photoelectrochemistry in fuel generation Reviews basic theory and best-known catalysts and best conditions/processes for fuel generation in each of the chapters Covers standard methodologies, processes, and limitations for large-scale applications Focusses on sustainable production of fuels from renewable energy and resources This book aims at graduate students/researchers in chemical, energy and materials engineering.

Photoelectrocatalysis: Fundamentals and Applications presents an in-depth review of the topic for students and researchersworking on photoelectrocatalysis-related subjects from pure chemistry to materials and environmental chemistry inorder to propose applications and new perspectives. The main advantage of a photoelectrocatalytic process is the mildexperimental conditions under which the reactions are carried out, which are often possible at atmospheric pressure androom temperature using cheap and nontoxic solvents (e.g., water), oxidants (e.g., O2 from the air), catalytic materials (e.g.,TiO2 on Ti layer), and the potential exploitation of solar light. This book presents the fundamentals and the applications of photoelectrocatalysis, such as hydrogen production fromwater splitting, the remediation of harmful compounds, and CO2 reduction. Photoelectrocatalytic reactors and lightsources, in addition to kinetic aspects, are presented along with an exploration of the relationship between photocatalysisand electrocatalysis. In addition, photocorrosion issues and the application of selective photoelectrocatalytic organictransformations, which is now a growing field of research, are also reported. Finally, the advantages/disadvantages andfuture perspectives of photoelectrocatalysis are highlighted through the possibility of working at a pilot/industrial scale inenvironmentally friendly conditions. - Presents the fundamentals of photoelectrocatalysis - Outlines photoelectrocatalytic green chemistry - Reviews photoelectrocatalytic remediation of harmful compounds, hydrogen production, and CO2 reduction - Includes photocorrosion, photoelectrocatalytic reactors, and modeling along with kinetic aspects